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氮磷硅系纳米凝胶阻燃剂的制备及表征PAGE\*MERGEFORMAT18目录TOC\o"1-3"\h\z\uHYPERLINK\l"_Toc6160759"1绪论PAGEREF_Toc6160759\h3HYPERLINK\l"_Toc6160760"1.1引言PAGEREF_Toc6160760\h3HYPERLINK\l"_Toc6160761"1.2阻燃剂的分类PAGEREF_Toc6160761\h3HYPERLINK\l"_Toc6160762"1.2.1卤系阻燃剂PAGEREF_Toc6160762\h4HYPERLINK\l"_Toc6160763"1.2.2氮系阻燃剂PAGEREF_Toc6160763\h5HYPERLINK\l"_Toc6160764"1.2.3磷系阻燃剂PAGEREF_Toc6160764\h5HYPERLINK\l"_Toc6160765"1.2.4硅系阻燃剂PAGEREF_Toc6160765\h6HYPERLINK\l"_Toc6160766"1.3阻燃机理PAGEREF_Toc6160766\h7HYPERLINK\l"_Toc6160767"1.4本课题的研究内容PAGEREF_Toc6160767\h8HYPERLINK\l"_Toc6160768"1.4.1本论文的研究背景PAGEREF_Toc6160768\h8HYPERLINK\l"_Toc6160769"1.4.2研究内容PAGEREF_Toc6160769\h9HYPERLINK\l"_Toc6160770"1.4.3研究创新点PAGEREF_Toc6160770\h9HYPERLINK\l"_Toc6160771"2氮硅系纳米凝胶阻燃剂的制备PAGEREF_Toc6160771\h10HYPERLINK\l"_Toc6160772"2.1实验仪器与材料PAGEREF_Toc6160772\h10HYPERLINK\l"_Toc6160773"2.1.1实验药品与试剂PAGEREF_Toc6160773\h10HYPERLINK\l"_Toc6160774"2.1.2实验设备PAGEREF_Toc6160774\h11HYPERLINK\l"_Toc6160775"2.2氮硅系纳米凝胶的合成PAGEREF_Toc6160775\h11HYPERLINK\l"_Toc6160776"2.2.1三羟甲基氨基甲烷、苯丙氨酸与TosOH合成中间产物PAGEREF_Toc6160776\h11HYPERLINK\l"_Toc6160777"2.2.2含氮硅阻燃剂的合成PAGEREF_Toc6160777\h12HYPERLINK\l"_Toc6160778"3氮磷硅系纳米凝胶阻燃剂的制备PAGEREF_Toc6160778\h13HYPERLINK\l"_Toc6160779"3.1实验仪器与材料PAGEREF_Toc6160779\h13HYPERLINK\l"_Toc6160780"3.2实验部分PAGEREF_Toc6160780\h13HYPERLINK\l"_Toc6160781"3.2.1去除氨基保护基TosOHPAGEREF_Toc6160781\h13HYPERLINK\l"_Toc6160782"3.2.2合成氮磷硅系纳米凝胶阻燃剂PAGEREF_Toc6160782\h13HYPERLINK\l"_Toc6160783"3.3本章小结PAGEREF_Toc6160783\h14HYPERLINK\l"_Toc6160784"4阻燃剂的表征及对比分析