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包渗工艺制备TiAl合金表面Si-Y共渗层的组织和抗高温氧化性能(英文) Title:MicrostructureandHigh-temperatureOxidationResistanceofSi-YCo-dopedSurfaceLayerProducedbyPackCementationTechniqueonTiAlAlloy Abstract: TiAlalloyshavegainedsignificantattentionintheaerospaceandautomotiveindustriesduetotheirremarkablehigh-temperaturemechanicalproperties.However,thepooroxidationresistancelimitstheirpracticalapplicationsatelevatedtemperatures.Inthisstudy,aSi-Yco-dopedsurfacelayerwaspreparedonaTiAlalloyusingthepackcementationtechnique.Themicrostructureandhigh-temperatureoxidationresistanceoftheSi-Yco-dopedsurfacelayerwereinvestigated. Introduction: TheSi-Yco-dopedsurfacelayerisapromisingtechniquetoenhancetheoxidationresistanceofTiAlalloys.SicanformaprotectiveSiO2scale,whileYcanstabilizetheoxidescalesandimproveadhesion.ThepackcementationtechniqueisaneffectivemethodtoachieveSi-Yco-dopingduetoitssimplicityandlowcost.Thisstudyaimstoinvestigatethemicrostructureandhigh-temperatureoxidationresistanceoftheSi-Yco-dopedsurfacelayeronTiAlalloy. ExperimentalProcedure: 1.PreparationofTiAlSubstrates:TiAlsampleswerecutintoappropriatesizesandpreparedbygrinding,polishing,andultrasoniccleaning. 2.PackCementationProcess:TheSi-Yco-dopedsurfacelayerwaspreparedbypackcementationusingYandSipowders. 3.HeatTreatment:TheTiAlsampleswithSi-Yco-dopedsurfacelayerwereheat-treatedinavacuumfurnaceat1000°Cfor5hours. 4.MicrostructuralCharacterization:ThemicrostructureoftheSi-Yco-dopedsurfacelayerwasexaminedusingscanningelectronmicroscopy(SEM)andX-raydiffraction(XRD). 5.High-TemperatureOxidationTest:TheSi-Yco-dopedTiAlsampleswereoxidizedathightemperatures(800-1000°C)foracertainperiodoftime.Theweightgainandoxidescalemorphologywereanalyzed. ResultsandDiscussion: TheSEMimagesrevealedthattheSi-Yco-dopedsurfacelayerexhibitedacompactmicrostructurewithoutvisiblecracksorpores.TheXRDanalysisconfirmedtheformationofTi-Si-Ycompounds,Ti5Si3,andY2O3phasesonthesurfacelayer.TheSi-Yco-dopedsurfacelayersignificantlyimprovedthehigh-temperatureoxidationresistanceoftheT