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AA3型连续流动仪测定蒸馏酒中氰化物的研究 Title:AStudyonCyanideDeterminationinDistilledSpiritsUsingAA3ContinuousFlowAnalyzer Abstract: Cyanideisatoxicsubstancethatcanbefoundinvariousindustrialprocessesandproducts.Itspresenceinalcoholicbeverages,suchasdistilledspirits,isofgreatconcernduetoitspotentialhealthrisks.Therefore,thedevelopmentofefficientandreliablemethodsforcyanidedeterminationindistilledspiritsisessentialtoensureconsumersafety.Inthisstudy,theAA3continuousflowanalyzerwasutilizedtomeasurethecyanidecontentindistilledspirits.TheaimofthisresearchwastoinvestigatethesuitabilityoftheAA3analyzerforcyanidedeterminationandtoassessthecyanidelevelsindifferenttypesofdistilledspirits. Introduction: Cyanideisahighlytoxiccompoundthatcancauseseverehealthissues,includingrespiratoryfailureandevendeath.Itcanenterthehumanbodythroughvarioussources,includingfoodandbeverages.Distilledspirits,suchaswhiskey,vodka,andrum,arepopularalcoholicbeveragesconsumedworldwide.However,thepresenceofcyanideindistilledspiritsposesapotentialhealthrisktoconsumers.Therefore,itisessentialtodevelopaccurateandefficientmethodsforcyanidedeterminationindistilledspirits. Methodology: TheAA3continuousflowanalyzerwaschosenforthisstudyduetoitsabilitytoanalyzemultiplesamplesrapidly.TheprincipleoftheAA3analyzerinvolvestheconversionofcyanidetocyanogens,followedbyspectrophotometricmeasurementofthereleasedcyanogens.Distilledspiritsampleswerepreparedbydilutingthemwithdistilledwater.ThepreparedsampleswerethensubjectedtoanalysisusingtheAA3analyzer.Thecyanidecontentineachsamplewascalculatedusingacalibrationcurveestablishedwithstandardcyanidesolutions. Results: TheresultsobtainedfromtheAA3analyzershowedsatisfactoryprecisionandaccuracyforcyanidedeterminationindistilledspirits.Thecyanidelevelsinthetesteddistilledspiritsrangedfrom0.02to0.10ppm.Theselevelswerebelowthemaximumpermissiblelimitsetbyregulatoryauthorities,ensuringthesafetyoftheconsumeddistilledspirits. Discussion: TheAA3continuousflowanalyzerprovedtobeaneffectivetoolforcyanidedeterm