环境空气—有机磷农药测定—气相色谱法.pdf

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FHZHJDQ0205环境空气有机磷农药的测定气相色谱法

F-HZ-HJ-DQ-0205
环境空气—有机磷农药的测定—气相色谱法

1范围
1.1本方法所列有机磷农药的检测限和最小检出浓度见表1。

表1有机磷化合物曲线范围、检测限和最低检出浓度
化合物名称工作范围检出限
英文名称中文名称大气浓度样品(1)进入柱内(2)进入柱内(2)样品(1)大气浓度(1)
（mg/m3）(µg/样品)的量（ng）的量（ng）(µg/样品)(mg/m3)
1.Azinphosmethyl谷硫磷0.02~0.62.4~721.2~360.060.20.001
2.Chlorpyrifos毒死稗0.02~0.62.4~721.2~360.020.040.0004
3.Diazinon地亚农0.01~0.31.2~360.6~180.020.040.0004
4.Dicrotophos百治磷0.025~0.753.0~901.5~450.10.20.002
5.Disulfoton乙拌磷0.01~0.31.2~360.6~380.020.040.0004
6.Ethion乙硫磷0.04~1.24.8~1442.4~720.020.040.0004
7.Ethoprop灭克磷0.01~0.31.2~360.6~180.020.040.0004
8.Fenamiphos克线磷0.01~0.31.2~360.6~180.070.140.001
9.Fonofos地虫磷0.01~0.31.2~360.6~180.020.040.0004
10.Malathion硫克磷1.0~3.012~3606~1800.050.10.001
11.Methamidophos甲胺磷0.02~0.62.4~721.2~360.30.60.005
12.Methylarathion甲基对硫磷0.02~0.62.4~721.2~360.020.040.0004
13.Mevinphos速灭磷0.01~0.31.2~360.6~180.060.20.001
14.Monocrotophos久效磷0.025~0.753.0~9.01.5~450.20.40.004
15.Parathion对硫磷0.005~0.150.6~180.3~90.020.040.0004
16.Phorate甲拌磷0.005~0.150.6~180.3~90.020.040.0004
17.Ronnel皮蝇磷1.0~3012~3606~1800.020.040.0004
18.sulprofos硫灭克磷0.1~3.012~3606~1800.030.060.0005
19.Terbufos特丁磷0.01~0.31.2~360.6~180.020.040.0004
（1）以采样体积120L时计算（流速1L/min采2h，0.5L/min采4h，0.4L/mi